Stack emission sampling

Dioxin, PCDD-PCDF and PCB sampling system compliant with UNI-EN 1948:2006

This sentence refers to the last variation of the version dated 1999 because it has been changed some phases in the technical-analytical process and there are new normative references about oxygen sampling (EN-14789) and humidity content (EN-14790).

The gas is sampled isokinetikally in the emission conduit. The PCDD/PCDF is absorbed by the particulate and present gaseous, recollected in the sampling line. The system gathering components may be a filter, a device for the recovery of the condensate and an absorbing material liquid or solid compatible with the chosen sampling system.

The regulations foresee choosing between three different sampling systems:

Filter/condenser method
Dilution method
Cooled sensor method

The first method is the most used one, contemplating the insert of a support for XAD-2 amberlyst resin or similar or purified polyurethane foam (PUF-Skc P226-131).

Filter/condenser method: the concept of the method is illustrated in the picture underneath.

tl_files/applicazioni/en_diossine_01.png

The system foresees that the filter is placed downstream of the nozzle after the heated sensor (outside of the conduit) in a specifical heated tank. The filter has to be maintained less than 125°C, over the gas dew point in the chimney. When it is foreseen a major load of dust it might be incorporated a quartz wool filter or a cyclone device in the sampling line before the filter, to avoid an overload of the same filter. Downstream, a condenser is connected to cool the sampled gas underneath 20°C. The device may be also used with a higher temperature only if the results obtained in the event have been demonstrated that are the same. Gaseous part of PCDD/PCDF aerosols are held back by the absorb solid. In a variant of the sampling system the solid absorbing element may be placed between the condenser and the gathering condensate device. The flux repartition system differs after filtration there is a flow distributor (similar to those used for other methods of emission sampling). The main high volume flow as to be compliant with the Isokinetic conditions (ISO-9096) crosses the filter. The secondary current after the repartition of the flux corresponds to the device with the condensation and absorbent unit previously described. The sampling must be performed according to the dictates and positioning indicated into the EN-13284 regulations.

Sampling time is anticipated in a range included between 6 and 8 hours, even if in the regulations refer to an average estimated sampling time 6h. The sampling system has been validated for high voltage flow between 0,5 m3/h and 0,7 m3/h (secondary current) and between 3 m3/h and 5 m3/h (main current). For the device with resin XAD-2 previously purified a quantity of circa 30g has been indicated. Regulate by-passed flow to maintain the ratio between the derived flow and the main flow (±10%); making sure that the speed in the XAD-2 cartridge is not greater than 34 cm/s.

Marking of the filtration device: mark the filter dividing into portions from 5 to 30 µl of solution of sampling reference on different points of the filter. Keep the filter vertical for a short period until the solvent is evaporated. The filter can be used for sampling only 2 hours after the reference marks have been applied. The marked filter may be stored for several days. In addition to that, also the absorbing material XAD-2 can be marked, or it might be marked in alternative to the filter. If during sampling need to replace the marked filter, the new one must be marked as the same time. This last option must be considered into final phases of the calculus.

Filter/condenser method: option with solid absorbent upstream of the condensate collector.

Sampling line is illustrated in the following picture.

tl_files/applicazioni/en_diossine_02_epa29.png

The gas from the conduit enters into the sampling line through a heated sensor containing a core and some parts in contacts with the glass sample. The filter holder is contained into an electrically heated box located downstream the sensor. This is followed by a water-cooled serpentine condenser and a cartridge also cooled with water and filled with XAD-2 resin. The condensate and the gas pass through resin and in a balloon flask in which condensate is recollected. The gas temperature in the sensor and in the filter is regulated between the dew point of the gas in the conduit and 120°C. In the sensor there is a thermocouple kind-K to check the gas temperature in the conduit and a Pitot tube kind S, to measure the flow voltage in the conduit. After the condensate collector the gas is aspirated by a pump through a drying line filled with silica gel, a gas meter and a flat orifice flow-measuring device. Sampling system is made on the base of a volume flow from circa 5 liters per minute to 25 liters per minute. All the elements included into sampling line not in contact with the sample are linked with rubber flexible tubes.

Materials needed for a correct dioxin sampling in complaint EN-1948:2006 Filter/Condenser/Resin XAD-2 method

Material needed for a correct dioxin sampling in complaint EN-1948-1:2006 and EPA 23. Solid resin absorber downstream gathering condenser XAD-2

Refill materials for dioxin sampling in complaint with EN-1948

INFORMATION TO CUSTOMERS ON THE PROCESSING OF PERSONAL DATA IN COMPLIANCE WITH ART. 13 OF THE EU 2016/679/ REGULATION PERSONAL DATA PROTECTION GENERAL REGULATION

Types of personal data

Dear Customer, AMS Analitica Srl, as Data controller, wishes to inform you that in performance of the contract, or of the formal agreements, personal data will be processed in compliance with the provisions of the Personal Data Protection General Regulation and with due respect for the obligations relating to correctness, lawfulness and confidentiality. The data undergoing processing refer to the personal data (Company name, address, VAT number, Iban code) of the Company as well as name, surname, address, email-PEC, telephone number, tax code of the persons representing the Company for legal, administrative and commercial activities.

Legal basis and purposes of the processing

The processing of personal data will be made for the following purposes :

order formulations, quotation requests, contracts concerning the sale of our the products and services;
administrative, accounting and contractual management of the existing legal relationship and relevant legal obligations ;
provision of defined products - services;
data filing aimed at the retention of accounting documents for the necessary time requested by the standards applicable ;
protection of the contractual rights of the undersigned company, even in the event of a dispute.
communications of commercial and promotional initiatives concerning the products - services provided or similar.

For the aforementioned purposes, the processing is necessary for the performance of the existing contract or of pre-contractual measures, implemented upon your request (aimed at, e.g., the negotiation of orders and quotations). The processing of your personal data for the above said purposes does not require express consent; any refusal to supply data may prevent us from continuing the contractual relationship.

For further purposes related to activities of advertising, promotional and commercial communication concerning new products and services, performed by phone, mailing or postal service, the Company shall process your data only after your express permission to do so.

Procedures of the processing and applied logics

The processing of personal data will be made through documents and paper files and/or by means of electronic and/or web tools in compliance with the provisions of the law guaranteeing the safety and secrecy of your data as well as the exactness, updating and relevancy of the data with respect for the purposes declared with the aim to avoid access and consequent processing of the data by unauthorized personnel. The logic applied when the data is processed with the use of electronic instruments, employed for the management of personal data aimed at the sale of products and provision of services, is based on the application of a specific policy limiting access to specifically authorized Company’s personnel. As far as possible, the Company applies the necessity principle which provides the configuration of computer systems and programs in order to minimize the use of personal and identification data so as to exclude their processing when the purpose of the specific activity can be achieved by using anonymous data or, respectively, suitable modes that allow identifying the person only in case of need.

Conservation period

Your personal data will be kept by the Data Controller as long as the legal relationship is established. The said data will only be used to fulfill legal obligations (such as preservation of accounting documents, storage of contract documents for any dispute or contractual liability) for a period of 10 years on expiry of which data will be erased or made anonymous.
For purposes relating to promotional, advertising or commercial activities of products and services other than those by you already purchased and used, your data will be kept until you inform us that you are no longer interested in receiving our communications for the above mentioned purposes.

Dissemination - Transfer availability and communication of data

Personal data shall not be disseminated or transferred to countries outside the EU. Apart from communications made to comply with statutory requirements, such as legal obligations and those foreseen by community rules and regulations, your personal data will be processed by employees and collaborators of the undersigned Data Controller in relation to the specific duties assigned and may be disclosed in Italy to public authorities or private institutions, to companies or professionals, credit institutions, subsidiaries and associated companies, data-processing and consulting companies, credit collection and insurance companies, professionals and companies providing consultancy services (e.g.: legal, fiscal, training and accounting services, etc.), to subjects who require to access the user’s data for the purpose mentioned above. All of them shall be provided by the undersigned Data controller of the information which is strictly necessary to achieve the aims for which personal data are collected; this would be done in full respect of the data confidentiality and protection.

Rights of the person concerned

With regard to these data and at any time, by sending simple written notice to the Data Controller even by email, directly and/or through a delegated person, you will be able to:

obtain access to personal data to know the origin of the data, the purposes of data processing, the logic applied to the processing through electronic media, data categories, recipients or categories of recipients of personal data to whom such data may be communicated, the conservation period of the data by the recipient, and their communication in an intelligible form;
obtain the correction, or supplementing of the information, the deletion of data, or the restriction of their processing;
object, on legitimate grounds, to the processing of your personal data ;
obtain data portability, where relevant ;
withdraw your consent at any time ;
lodge a complaint with a supervisory authority.

The above mentioned rights shall be exercised in accordance with the procedures and provisions of the reference regulations.

PERSONAL DETAILS OF DATA CONTROLLER

Data controller of the processing is the company AMS Analitica with registered office in Italy - Pesaro, Ple Coralloni, 12 – email info@amsanalitica.com – Ph +39 0721 26243

information to SUPPLIERS on the processing of personal data in compliance with art. 13 of the EU 2016/679/ regulation personal data protection general regulation

Types of personal data

Dear Supplier, AMS Analitica Srl, as Data controller, wishes to inform you that in performance of the contract, personal data will be processed in compliance with the provisions of the Personal Data Protection General Regulation and with due respect for the obligations relating to correctness, lawfulness and confidentiality. In particular, corporate data will be processed (Company name, address, VAT number, Iban code) and the data of your directors, managers, employees and collaborators involved in the present business dealings, as name and surname, email, phone number, that you communicated us during pre-contract negotiations. Additionally, VAT and Tax number as well as any registration number of professionals will be processed.

Legal basis and purposes of the processing

The processing of personal data will be made for the following purposes:

order formulations, quotation requests, contracts concerning the products and services requested;
administrative, accounting and contractual management of the existing legal relationship and relevant legal obligations ;
performance of the contract ;
data filing aimed at the retention of accounting documents and at the protection of the contractual rights of the undersigned company, even in the event of a dispute.

For the aforementioned purposes, the processing is necessary for the performance of the existing contract or of pre-contractual measures taken on your request and aimed at, e.g., the negotiation of orders and quotations. The processing of your personal data for the above said purposes does not require express consent. Any refusal to supply data may prevent us from continuing the contractual relationship.

Procedures of processing applied logics and conservation period

The processing of personal data will be made through documents and paper files and by means of electronic and/or web tools in compliance with the provisions of the law guaranteeing the safety and secrecy of your data as well as the exactness, updating and relevancy of the data with respect for the purposes declared with the aim to avoid access and consequent processing of the data by unauthorized personnel.
Personal data shall be preserved by the undersigned Data controller throughout the duration of the relationship and for a period of ten years following termination of the aforementioned relationship, for legal or legislative obligations (such as conserving accounting documents, storing contract documents for any contentious procedure or contractual liabilities). On expiry of that period, data will be cancelled or made anonymous.

communication and sharing of data

Personal data shall not be disseminated or transferred to countries outside the EU. Apart from communications made to comply with statutory requirements, such as legal obligations and those foreseen by community rules and regulations, the personal data of the supplier may be disclosed in Italy to public authorities or private institutions, to companies or professionals providing IT consultancy services, consultancy services on organizational management, legal and accounting services, who require to access the user’s data for the purpose mentioned above. All of them shall be provided by the undersigned Data controller of the information which is strictly necessary to achieve the aims for which personal data were collected; this would be done in full respect of the data confidentiality and protection. Some of these categories of persons use the data for the same means as defined above in their capacity as independent Persons in Charge. The list of the subjects or the subject categories to whom the personal data can be communicated or that can get to know them as appointed representative is at your disposal at the premises of the data controller.

Availability of data

The subjects or the subject categories who can access your personal data, in the capacity of data processors or persons in charge of processing the said data, and within the sphere of their respective functions for the performance of their tasks and in accordance with the instructions received, are the employees of AMS Analitica specifically authorized to handle this data for the fulfillment of the aforementioned purposes.

Diritti dell'interessato

With regard to these data and at any time, by sending simple written notice to the Data Controller even by email, directly and/or through a delegated person, you will be able to:

obtain access to personal data to know the origin of the data, the purposes of data processing, the logic applied to the processing through electronic media, data categories, recipients or categories of recipients of personal data to whom such data may be communicated, the conservation period of the data by the recipient, and their communication in an intelligible form;
obtain the correction, or supplementing of the information, the deletion of data, or the restriction of their processing;
object to the processing of your personal data ;
obtain data portability, where relevant ;
withdraw your consent at any time ;
lodge a complaint with a supervisory authority.

The above mentioned rights shall be exercised in accordance with the procedures and provisions of the reference regulations.

PERSONAL DETAILS OF DATA CONTROLLER

Data controller of the processing is the company AMS Analitica with registered office in Italy - Pesaro, Ple Coralloni, 12 – email info@amsanalitica.com – Ph +39 0721 26243

Code	Article
600/SIR1500BB	Isokinetic heated probe with rear box 1500mm
600/DX100101K	Cooling device support with rear mount
600/DX10011948S	Refrigerant set with XAD bottle, trap and fittings
600/SF001KDZ	Stack Frost Refrigerant System for Dioxin sampling
600/CRS050K	37 mm glass thimble holder complete with metal ring nut
600/TF200	TermoFlow 200 thermoregulation device
600/SUV6/8	Glass nozzle set 6-8-10mm (1+1+1)
600/GFR001	Heated probe attachment group
600/TVSR1500ST*	Nozzle attachment set in glass complete w nozzle and linking
600/CCTFSIR4	Heated probe connection cable 4mt
600/CCTFSIR8	Heated probe connection cable 8mt
600/CRS029	47 mm glass filter holder for direct sampling
600/CRS029D	47 mm glass filter holder for derived sampling
600/TGS001K	Silica gel trap w quick inlets
600/VT001T	Thermal container for condensate gather

Code	Article
600/SIR1500BB	Isokinetic heated probe w rear box 1500mm
600/DX100101K	Cooling device support w back mount
600/DX0005G	XAD-2 GL45/25 trap w 35 baffle and cladding
600/SF001KDZ	Stack Frost refrigerant system for dioxin sampling
600/SF002MSL	Refrigerated tank combined w StackFrost device
600/CRS050K	37mm glass thimble holder complete w metal ring nut
600/TF200	TermoFlow200 Thermoregulation device
600/SUV6/8	Glass nozzle set 6-8-10mm (1+1+1)
600/GFR001	Heated Probe attachment group
600/TVSR1500ST*	Glass nozzle attachment set complete w nozzles and linking
600/CCTFSIR4	Heated probe connection cable 4mt
600/CCTFSIR8	Heated probe connection cable 8mt
600/CRS029	47 mm glass filter holder for direct sampling
600/CRS029D	47 mm glass filter holder for derived sampling
600/TGS001K	Silica gel trap w quick inlets
600/SGDX23001K	5 gas bubblers set and fittings for method 1948 and EPA 23

Code	Article
NFS/GF1-47-100	47mm GF1 grade glass fiber (Eq GFA) pckg 100pcs
SK/225-1823	Tissuquartz™ quartz fiber filter thick.432µ 47mm pckg.25 pcs
PL/TBD7212	Glass fiber filter membrane clad in PTFE max.300°C 47mm pckg.50 pcs.
600/CN086R25	Thimbles in borosilicate 30x80 pckg.25pcs
600/CN088R25	Thimbles in pure silica HT Max.1000°C 30x80 pckg.25 pcs.
600/HI39P503F2	Quartz wool for baskets 500g
SK/P226201	XAD-2 SKC resin for PCDD/PCDF 100g EN-1948-1
SK/P226131	SKC non-purified polyurethane foam pckg.10 pcs
SK/P226131C	SKC pre-conditioned polyurethane foam pckg.10 pcs

Stack emission sampling

Materials needed for a correct dioxin sampling in complaint EN-1948:2006 Filter/Condenser/Resin XAD-2 method

Material needed for a correct dioxin sampling in complaint EN-1948-1:2006 and EPA 23. Solid resin absorber downstream gathering condenser XAD-2

Refill materials for dioxin sampling in complaint with EN-1948

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INFORMATION TO CUSTOMERS ON THE PROCESSING OF PERSONAL DATA IN COMPLIANCE WITH ART. 13 OF THE EU 2016/679/ REGULATION PERSONAL DATA PROTECTION GENERAL REGULATION

Types of personal data

Legal basis and purposes of the processing

Procedures of the processing and applied logics

Conservation period

Dissemination - Transfer availability and communication of data

Rights of the person concerned

PERSONAL DETAILS OF DATA CONTROLLER

information to SUPPLIERS on the processing of personal data in compliance with art. 13 of the EU 2016/679/ regulation personal data protection general regulation

Types of personal data

Legal basis and purposes of the processing

Procedures of processing applied logics and conservation period

communication and sharing of data

Availability of data

Diritti dell'interessato

PERSONAL DETAILS OF DATA CONTROLLER